Agilent Technologiesメーカー5975の使用説明書/サービス説明書
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Agilent T echnologies 5975 Series Mass Selective Detectors Site Preparation Guide 5975 Series Site Prep.book Page 1 Thursday, January 31, 2008 9:47 AM.
Site Prepar ation Guide Notices © Agilent T e chnologies, Inc. 2008 No part of this manual ma y be reproduc ed in any form or by any means (including elec- tronic storage and retrieval or translation into a foreign language) without prior agree- ment and written consent from Agilent T echno logies, Inc.
Site Preparation Guide 3 Conten ts 1 General Inf ormati on Instrument I dentificati on 6 5975 MSD vers ions 6 Important Safety Warnings 7 Many inte rnal part s of the M SD carry d angerous voltages 7 .
4 Site Prepar ation Guide V oltage ran ges of ma jor comp onents 23 Power co nfig urat ions 24 Power re quiremen ts 25 Power pl ugs and cor d 2 6 Other electri cal consid eratio ns 27 Air Condi tio ni.
5 5975 Series Mass Selective Detectors Site Preparation Guide Agilent T echnologie s 1 Genera l Infor mati on Instrume nt Id entifi cation 6 Import ant Safety W arnings 7 Hydrog en Sa fety 9 Chemical .
6 Site Prepar ation Guide General In formation Instrument Identification Each 5975 Series Mass Selectiv e Detector ( MSD) is identified by a unique 10-character serial number . This serial number is located on a label on the low er lef t side nea r th e front of the instr u ment.
General Informati on Site Preparation Guide 7 Important Safety W arni ngs Bef ore mo ving on , there are sev eral im port ant saf ety noti ces that y ou should alwa y s k eep in mind when using the 5975 Series M ass S elective D etector .
8 Site Prepar ation Guide General In formation The use of incorrect or makeshift fuses or the shor t-circuiting of fuse holders creat es a shock ha zard f or t he operator an d can damage t he inst ru ment. Replac e fuse s only wit h fuse s of iden tical cu r rent rati ng and type.
General Informati on Site Preparation Guide 9 Hydrogen Safety Hydrogen gas may be used as car rier gas , and/or as fuel for cer t ain G C detec tors. When mixed wit h air , hydrogen can form ex plosive mixt ures. A detaile d discussion of h y drogen safety appears in Chapt er 1 of the Agile nt 5975 MSD Troubleshooting and Maintenance Manual.
10 Site Prepar ation Guide General In formation Chemical Safety W A RNING The foreline pump exhaust and split vent exhaust will con tain traces of the chemicals you are analyzing. These could potentially be toxic. V ent the foreline pump exhaust and spl it vent exhaust outside your labora tory or into a fume hood.
General Informati on Site Preparation Guide 11 Safety and Regulatory Cer tifications The 5975 Series M SD conf o rms to the follo wing saf ety standards: • Canadian Standards Associ a tion (CSA): C AN/CSA–C22.
12 Site Prepar ation Guide General In formation Symbols W arn ings in the man ual or on the instrument mu st be obse rve d during a ll phase s o f ope rat ion, ser vice , an d rep air of th is inst r umen t. F ailu re t o c omply with thes e precau tions violat es s afety st and ards of de sign and t he i nte nded use of the in str umen t.
General Informati on Site Preparation Guide 13 Electromagnetic compatibility This device complies with t he requiremen ts of CISPR 11. Operat ion is subject to the f ollo wing tw o cond itions: • This de vice ma y not caus e harmful interfer ence.
14 Site Prepar ation Guide General In formation Cleaning T o clean the unit, dis connect the po wer and wipe do wn wit h a dam p, lint- free cloth. Recycling the Produc t F or recyclin g, cont act y our local Agilen t sales office. 5975 Series Site Prep.
15 5975 Series Mass Selective Detectors Site Preparation Guide Agilent T echnologie s 2 Site Preparation Overview 16 Space and W eight Requireme nts 20 Communi cation s Requireme nts 22 Electr ical Re.
16 Site Prepar ation Guide Site Preparation Overview Bef ore the 5975 Series MSD system can be installed, the sit e must be properly prepa red. Site preparat ion include s, but is not li mited to, ensur ing that adequat e facili ties are available. Among th e site requ irement s are: • A dequat e space is available for t he MSD system .
Site Preparation Site Preparation Guide 17 • Com plying with all local la ws (co des, ord inances, and regu lation s) f or mechan ical, build ing, and elec trical distr ibuti on systems, hazar dous was t e disposa l, an d chemi cal s tora ge. Compliance must exist prior to installation.
18 Site Prepar ation Guide Site Preparation Ag ilent Technolo gies is not re sponsi ble for: • Any task n ot list ed in t he 5975 Series MSD T roubleshooting and Main te nanc e Man ual or the inst a.
Site Preparation Site Preparation Guide 19 Other documentat ion Additiona l infor matio n is co nt ained in t he following docum ent at ion: • 5975 Series MSD T roubleshooting and Maintenance Manual • 5975 Series MS D Operation man ual • 6890 Series GC manuals • GC acce ssories (autosam pler , etc.
20 Site Prepar ation Guide Site Preparation Space and W eight Requi rements Table 2 l ists dim ensi on an d weight infor mat ion for t h e MS D and rel ate d component s. Y our sit e must have enough benc h space for the MSD , GC, dat a system, a nd accessor ies (Figur e 1).
Site Preparation Site Preparation Guide 21 Ta b l e 2 Product dimens ions Approxima te Dimension s, cm (in) Produc t Heigh t Width Dept h W eight , kg ( lb) 5975 Seri e s MSD • G3170A D iffusion EI .
22 Site Prepar ation Guide Site Preparation Communication s Require ments Te l e p h o n e A tel ephone with a cord long enough t o be used at t he computer wil l allow the MSD ope r ator to commun icate with Agilen t Tech nologi es support personne l.
Site Preparation Site Preparation Guide 23 Electrical Requirements Y ou are res ponsible f or pro vidin g appr opriate elec trical po we r and po wer outlets f or all of the components in y our 5975 Series MSD system.
24 Site Prepar ation Guide Site Preparation Power configurations Electrical po wer for th e MSD must be single-phas e. The neutral wire cannot be used for safety grounding. The g round wire should car r y zero current ex cept for ground-fau lt cu rren t or st a tic elec tric d ischarge.
Site Preparation Site Preparation Guide 25 Power requirements Table 4 lists the po we r requirements f or t he 5975 Series MSD a n d related equipme nt. Extra po wer cap acity for future additio n s is rec ommended. Each pro duct listed r equir es a d edicated c ircuit.
26 Site Prepar ation Guide Site Preparation Power plugs and cord The MSD is supplied with a po w er cord and plug appropri ate f or the country from which t he order ori ginates.
Site Preparation Site Preparation Guide 27 Other electr ical considerat ions Additional electrica l consi deratio ns in clude: • Elec troma gnetic interfe renc e (EMI), such as is genera ted by NM Rs, radi o transmit ters, an d microwa ve link s, may inter fere with system perform ance.
28 Site Prepar ation Guide Site Preparation Air Conditioning and Envir onmental Requi rements Air co ndit ionin g cons idera tions inclu de t emperat ure, hu midi ty , air bor ne dust , and exhau st venting. Eac h of thes e is consid ered in more det ai l in the fol low i n g m a t e r i a l .
Site Preparation Site Preparation Guide 29 Airborne dust Agilent T echnolog ies recommends a ma ximum ai rborne particle dens ity of 55 μ g/m 3 . If y ou suspect y our site ex ceeds this l imit, co nt act y our local Agilen t T e chnologi es Cust omer Se rvice Organ ization.
30 Site Prepar ation Guide Site Preparation See your GC manu als for inform atio n on venting t he spli t vent. Fume (exhaust) hood An auxili ar y work space and fume hood are ne eded for some maint enance procedures.
Site Preparation Site Preparation Guide 31 Carrier and Reag ent Gas Requirements Table 6 list s the spec if ication s for the carr ier and reag ent gases. Pressur es and f l o ws a re as m easur ed at the bulkhe ad f itt ings on t he bac k of t he instr umen t, not at t he g as suppl y.
32 Site Prepar ation Guide Site Preparation Regulators, tubing, and fittings Y ou must supply appropriat e regulators for you r car rier and reagen t gas. • Regula tors m ust be dual-s ta ge. • Regul ators must hav e stainless -steel ( not e lastomer ic) diaphr agms.
Site Preparation Site Preparation Guide 33 Laboratory Suppl y Requirements Laborator y supply requirements vary wit h applicati ons. Cleaning solvents Cleaning t ask s for the M SD require t he follow.
34 Site Prepar ation Guide Site Preparation Spare parts a nd consumables The supplies and par ts list ed in Table 7 are used in the operati on and maintenance of a 5975 Series MSD sy stem. K eeping these parts on hand can reduc e sys tem do wntime r elate d to ins tr ument ma intenance an d repair .
Site Preparation Site Preparation Guide 35 Chemical Consu mables PF TBA (EI calib ration fluid) 05971-6 0571 PFDTD (CI calib ration fluid ) 8500-8130 EV AL A (eva luation sa mple) 05990-60045 OFN (Octafluor onapthalene) 5188-5348 OFN 100 fg/µL 5188-5347 Benzop h enone 85 00-5440 PFHT 5188-53 57 Foreline pump oil, P3, 0.
36 Site Prepar ation Guide Site Preparation 0.5-mm id , 85% V espel 15% graphite, for 0.32-mm id colum ns 5062-3506 0.8-mm id , 85% V espel 15% graphite, for 0.53-mm id colum ns 5062-3538 GC in let 0.27-mm id, 90% V espel 10 % graph ite, for 0. 10-mm id colum ns 5062-3518 0.
Site Preparation Site Preparation Guide 37 Receiving t he System When you r MSD sys tem is d elivere d, it is your resp onsi bilit y t o provide for remo val of the ship ping containers fr om the truck and thei r storage until inst al lation.
38 Site Prepar ation Guide Site Preparation Storage It is your respo nsibi lity to store the c ont ainer s unti l inst al lation . If your site does no t hav e adequat e st orage spac e, the c ont ainers may be stored at your expense i n a b onded wa rehouse.
Site Preparation Site Preparation Guide 39 Installation and V erification Installation Once the in stallatio n has beg un, it sho uld pro gress in a time ly manner to completion. D elays due t o inad equat e site preparation could c ause loss of instr ument use d uring t he warrant y period.
40 Site Prepar ation Guide Site Preparation Sensitivity specifications See the appro priate sensit ivity specifications f or your inst rument type. See the Agile nt T echnolo gies W eb site at http://www .agilent .com/ch em. NOTE SIM performance verification is not perf ormed at inst allation and must be purchased if desir ed.
41 5975 Series Mass Selective Detectors Site Preparation Guide Agilent T echnologie s A Power Cords This appendix sho ws t he pow er cords availabl e for the 5975 Series MSD. See page 26 for inf or mation a bout ensuring that the correct po wer cord is s upplied wit h your syst em .
42 Site Prepar ation Guide Power Cords Denm ark/Gr eenla nd, IEC 309 (Pa rt num ber 8120 -399 7) Austr alia/New Ze aland, AS 31 12-198 1 (Part numbe r 8120-136 9) India/S outh Africa , BS 546 (Par t numb er 8120 -4211) Israe l, SI 32 (Par t number 8120-5 182) Japan, NEMA L6-20 P (Part number G2025-601 89) 5975 Series Site Prep.
5975 Series Site Prep.book Page 43 Thursday, January 31, 2008 9:47 AM.
Agilent T echnologie s © Agilent T echnologies, Inc . Printed in USA, J a nuary 2008 5975 Series Site Prep.book Page 44 Thursday, January 31, 2008 9:47 AM.
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