A&DメーカーMS-70の使用説明書/サービス説明書
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ふ MS-70 MX-50 MF-50 ML-50 W M+PD4 000477D.
1. 1. 1. 1. This manual and Marks This manual and Mark s This manual and Mark s This manual and Mark s All safety messag es are iden tified by the fol low ing, “ WA R N I N G ” or “ CAUT ION ”, of ANSI Z535. 4 (Am erican N ational S tandar d Institute : Produc t Sa fety Sig ns and Labels) .
MS-70 / MX-50 / MF-50 / ML-50 1 Contents Contents Contents Contents 1. Safety an d Comp liance .................................................................. 3 2. Precaut ions .......................................................................
MS-70 / MX-50 / MF-50 / ML-50 2 8. Check Func tion ........................................................................... 41 8.1. Self-Check Function....................................................................... 41 8.1. 1. Op eration ...
MS-70 / MX-50 / MF-50 / ML-50 3 2. 2. 2. 2. Safety Safety Safety Safety and Compliance and Compliance and Compliance and Compliance WA R N I N G Do not use a sampl e that c ould mak e a da ngerous ch emical reactio n and ca use an explosi on or poi sonous gas, w hen the sampl e is dr ied.
MS-70 / MX-50 / MF-50 / ML-50 4 Compliance wit h FCC Rules Compliance wit h FCC Rules Compliance wit h FCC Rules Compliance wit h FCC Rules Please not e that t his dev ice g enerates, uses and can r adiate ra dio frequency energy .
MS-70 / MX-50 / MF-50 / ML-50 5 3. 3. 3. 3. Prec Prec Prec Precauti ons autions autions autions 3.1. 3.1. 3.1. 3.1. Install ing the Ana lyzer Install ing the Anal yz er Install ing the Anal yz er Inst.
MS-70 / MX-50 / MF-50 / ML-50 6 3.2. 3.2. 3.2. 3.2. During Use During Use During Use During Use --- --- --- --- C aution for M Caution for M Caution for M Caution for M easure easure easure easure ment Sa ment Sa ment Sa ment Sa f e ty fety fety fety --- --- --- --- Operate the a naly zer using the follow ing pr ocedure.
MS-70 / MX-50 / MF-50 / ML-50 7 Caution for Heating (Drying). W hen th e dryin g te mpe rat u re is set to 200 °C an d mea surem ent is sta r ted, the thermost at of the halog en lamp may work after 30 minut es. W he n th e halog en lamp has cooled down, t he nex t measure ment can be st arte d.
MS-70 / MX-50 / MF-50 / ML-50 8 4. 4. 4. 4. Outline and Outline and Outline and Outline and Features Feature s Feature s Feature s The moisture ana lyzer is bu ilt using a s upe r h ybri d s ensor ( S .H .S.) ad opt ed i n an analytical balance. Therefore, th e result is mo re precise and gets greater repeatability .
MS-70 / MX-50 / MF-50 / ML-50 9 The analy zer i s equi pped with a ser ial in ter face as st andard . It can be con nected to a printer or co mputer . The analy zer can cal ibrate th e wei ghing sensor (Use speci al mass .) and dry ing temperat ure (Use t emperatur e calibrator for MS- 70 and MX -50 ex cept MF- 50 and ML-50).
MS-70 / MX-50 / MF-50 / ML-50 10 5. 5. 5. 5. Packing List and Names of each part Packing List and Names of each part Packing List and Names of each part Packing List and Names of each part Keep the p acking b ox to m ove the an alyz er .
MS-70 / MX-50 / MF-50 / ML-50 11 All Accessories All Accessories All Accessories All Accessories Caution Please confirm th at th e analy zer is correct f or your local v olt age, recept acle type and po w e r cord.
MS-70 / MX-50 / MF-50 / ML-50 12 5.1. 5.1. 5.1. 5.1. Di spl ay a nd Key s Dis pl ay an d Key s Dis pl ay an d Key s Dis pl ay an d Key s Name S tate and Meaning At gram displa y Pr eset time is displa.
MS-70 / MX-50 / MF-50 / ML-50 13 #1 ML-50 can sel ect "s ta ndar d dryi ng " and "qui ck dryi ng" only . #2 ML-50 does not display "heating patt er n" .
MS-70 / MX-50 / MF-50 / ML-50 14 6. 6. 6. 6. Preparation Preparation Preparation Preparation s s s s 6.1. 6.1. 6.1. 6.1. Install ing the Ana lyzer Install ing the Anal yz er Install ing the Anal yz er Install ing the Anal yz er 1. Select the place to i nstall the analyz er .
MS-70 / MX-50 / MF-50 / ML-50 15 6.2. 6.2. 6.2. 6.2. Setting the Clock and C Setting the Clock and C Setting the Clock and C Setting the Clock and C alendar alend ar alend ar alend ar.
MS-70 / MX-50 / MF-50 / ML-50 16 6.3. 6.3. 6.3. 6.3. Proper Oper ati on for Prec isi on Mea sure ment Proper Oper ati on for Prec isi on Mea surement Proper Oper ati on for Prec isi on Mea surement Proper Oper ati on for Prec isi on Mea surement 6.3.1.
MS-70 / MX-50 / MF-50 / ML-50 17 6.3.3. 6.3.3. 6.3.3. 6.3.3. The Glas s Fibe r Shee t The Gl ass Fi ber Sh eet The Gl ass Fi ber Sh eet The Gl ass Fi ber Sh eets s s s Use the glass fiber sheet to measure the moisture content that is included in the following sampl es.
MS-70 / MX-50 / MF-50 / ML-50 18 7. 7. 7. 7. Measurement Pr ocedure Measurement Procedure Measurement Procedure Measurement Procedure 7.1. 7.1. 7.1. 7.
MS-70 / MX-50 / MF-50 / ML-50 19 1. T urn on the analyzer . The gr am unit (o f w eighing mode) i s dis played. Enter the St andard Mode Enter the St andard Mode Enter the St andard Mode Enter the St andard Mode 2 . Press the SELECT key to di splay an ana lysi s mode and press the ↓ or ↑ key to se lect 5td .
MS-70 / MX-50 / MF-50 / ML-50 20 1 1. Open th e heat er cov er . Put in a sampl e using the level indicator . Caution The sample needs t o be more than 0.1 g. Spread the sample ev enly. 12. If the ↑ key is pre ssed d u r i n g g r am d i sp la y , a n a ly s i s mode, measur e me nt u nit and mini m um scale v al ue are display ed.
MS-70 / MX-50 / MF-50 / ML-50 21 7.2. 7.2. 7.2. 7.2. Quick Mode Op erati o n Quick Mode Opera tion Quick Mode Opera tion Quick Mode Opera tion The quick mode can ob tain the moisture conten t with settings of A CCURACY and dryin g temperature.
MS-70 / MX-50 / MF-50 / ML-50 22 1. T urn on the analyzer . The gr am unit (o f w eighing mode) i s dis played. Enter the Q u ic k Mode Enter the Q u ic k Mode Enter the Q u ic k Mode Enter the Q u ic k Mode 2. Press the SELECT ke y to disp lay an anal ysis mode and press the ↓ or ↑ key to se lect quc .
MS-70 / MX-50 / MF-50 / ML-50 23 1 1. Open th e heat er cov er . Put in a sampl e using the level indicator . Caution The sample needs t o be more than 0.1 g. Spread the sample ev enly. 12. If the ↑ key is pre ssed d u r i n g g r am d i sp la y , a n a ly s i s mode, measur e me nt u nit and mini m um scale v al ue are display ed.
MS-70 / MX-50 / MF-50 / ML-50 24 7.3. 7.3. 7.3. 7.3. Progra m Nu mber Prog ra m Nu mbe r Prog ra m Nu mbe r Prog ra m Nu mbe r T he measurement conditions of all program numbers are set to the standard mode at the factory . The analyze r can s tore and re call proper ind ividual sett ings for each samp le with the program number (PROG No.
MS-70 / MX-50 / MF-50 / ML-50 25 8. 8. 8. 8. Measurement Measurement Measurement Measurement Programs Program s Programs Program s 8.1. 8.1. 8.1. 8.1. Lis t o f Lis t of Lis t of List of Measu rement Measu rement Measu rement Measu rement Progr ams Pro gram s Pr ogra ms Pro gram s There are five anal ysi s modes.
MS-70 / MX-50 / MF-50 / ML-50 26 8.1.1. 8.1.1. 8.1.1. 8.1.1. ACCURACY of the Standard Mode and Q uick Mode ACCURACY of the Standar d Mode and Q uick Mode ACCURACY of the Standar d Mode and Q uick Mode ACCURACY of the Standar d Mode and Q uick Mode ACCURACY of measurement can be set eithe r HI , MID.
MS-70 / MX-50 / MF-50 / ML-50 27 8.1.2. 8.1.2. 8.1.2. 8.1.2. Analyzing mo de of the A utomatic Mode Analyzing mo de of the Automatic Mode Analyzing mo de of the Automatic Mode Analyzing mo de of the Automatic Mode W hen the change of moisture content per one minute is less than the preset v alue, the measurement is automatically completed.
MS-70 / MX-50 / MF-50 / ML-50 28 How to Sele ct quic k mode (Extr acts) How to Sele ct quic k mode (Extr acts) How to Sele ct quic k mode (Extr acts) How to Sele ct quic k mode (Extr acts) Press the SELECT key during the gram dis play . Displ ay quc using the ↓ or ↑ ke y .
MS-70 / MX-50 / MF-50 / ML-50 29 8.2. 8.2. 8.2. 8.2. Procedures to Sto re a M easurement P rogram Procedu res to Store a M easurement P rogram Procedu res to Store a M easurement P rogram Procedu res to Store a M easurement P rogram 8.2.1. 8.2.1. 8.2.
MS-70 / MX-50 / MF-50 / ML-50 30 Select an Analysis Mode Select an Analysis Mode Select an Analysis Mode Select an Analysis Mode 5 . Pre ss the SELECT ke y to s e l e c t a s ymbol, it wi ll blink. Select an analysis mode usin g the ↓ or ↑ key . I f standard mode is used, se lect 5td .
MS-70 / MX-50 / MF-50 / ML-50 31 Set Set Set Set the Minimum Scale Value of th e Gram Display the Minimum Sca le Value of th e Gram Display the Minimum Sca le Value of th e Gram Display the Minimum Sca le Value of th e Gram Display 13. S e l e c t gr am display w i t h t h e SELECT key .
MS-70 / MX-50 / MF-50 / ML-50 32 8.2.2. 8.2.2. 8.2.2. 8.2.2. Ramp Drying Ramp Drying Ramp Drying Ramp Drying Sta nd ar d Sta nd ar d Sta nd ar d Standard Mode, Automati c Mode or Mode, Autom atic Mode.
MS-70 / MX-50 / MF-50 / ML-50 33 Select an Analysis Mode Select an Analysis Mode Select an Analysis Mode Select an Analysis Mode 5 . Pre ss the SELECT k e y to s e le c t a symbo l, it wil l blink. Select an ana lysis mode u sing the ↓ or ↑ key . I f standard mode is used, se lect 5td .
MS-70 / MX-50 / MF-50 / ML-50 34 Store Parameters and Finish t he Operation Store Parameters and Finish t he Operation Store P arameters and Finish th e Operation Store Parameters and Finish t he Operation 14. Press the ENTER key to store th e new para meters o f the measur ement pr ogram to pr ogram numbe r 3.
MS-70 / MX-50 / MF-50 / ML-50 35 Select an Analysis Mode Select an Analysis Mode Select an Analysis Mode Select an Analysis Mode 5 . Press the SELECT key to select a sy mbol, i t will bli nk. Se l e c t U-t of the ti mer mode w ith the ↓ or ↑ key .
MS-70 / MX-50 / MF-50 / ML-50 36 8.2.3. 8.2.3. 8.2.3. 8.2.3. Step Drying Step Drying Step Drying Step Drying Standard Mode, Automati c Mode or Standard Mode, Automati c Mode or Standard Mode, Automati.
MS-70 / MX-50 / MF-50 / ML-50 37 Select an Analysis Mode Select an Analysis Mode Select an Analysis Mode Select an Analysis Mode 5 . Pre ss t he SELECT ke y to b l i n k a s ymbo l, it will blink. Select an analysis mode usin g the ↓ or ↑ key . I f standard mode is used, se lect 5td .
MS-70 / MX-50 / MF-50 / ML-50 38 Set the Minimum Scale V alue of the % Dis play Set the Minimum Scale V alue of the % Dis play Set the Minimum Scale V alue of the % Dis play Set the Minimum Scale V alue of the % Dis play 13. S e l e c t t h e % display w i t h t he SELECT key .
MS-70 / MX-50 / MF-50 / ML-50 39 1. Display gram uni t (o f the wei ghing mode). Select a Pro gram Number to Edi t the Measure ment Select a Pro gram Number to Edi t the Measure ment Select a Pro gram Number to Edi t the Measure ment Select a Pro gram Number to Edi t the Measure ment Progr am Progr am Progr am Progr am 2.
MS-70 / MX-50 / MF-50 / ML-50 40 Set t Set t Set t Set the he he he Measurem ent Meas urem ent Measur ement Meas urem ent Uni t Unit Unit Unit 1 1 . Select mea surement u n i t with the SELECT key . Select the moistur e co ntent (bas ed on w et s a m pl e ) with the ↓ or ↑ ke y .
MS-70 / MX-50 / MF-50 / ML-50 41 9. 9. 9. 9. Check Function Check Function Check Function Check Function 9.1. 9.1. 9.1. 9.1. Self Self Self Self- - - -Check Function Check Function Check Function Check Function Use the s el f-check functi on to c heck w hether there i s an er ror or i naccurate result .
MS-70 / MX-50 / MF-50 / ML-50 42 9.2. 9.2. 9.2. 9.2. Test Sample (S Test Sam ple (S Test Sam ple (S Test Sam ple (Sodium odium odium odium T T T Ta rt ra te artr ate artr ate artr ate D D D Di hy d r .
MS-70 / MX-50 / MF-50 / ML-50 43 10. 10. 10. 10. Connecting to a Printer Connecting to a Printer Connecting to a Printer Connecting to a Printer Th e analy zer can be connected to a c ompact dot- matrix printer (AD-8121B) usi ng the RS-23 2C int erface.
MS-70 / MX-50 / MF-50 / ML-50 44 10.1. 10.1. 10.1. 10.1. Print sa mp les Print sa mp les Print sa mp les Print sa mp les 10.1.1. 10.1.1. 10.1.1. 10.1.1.
MS-70 / MX-50 / MF-50 / ML-50 45 10.1.2. 10.1.2. 10.1.2. 10.1.2. Example To Print Selected Items Example To Print Selected Items Example To Print Selected Items Example To Print Selected Items This pr.
MS-70 / MX-50 / MF-50 / ML-50 46 Print E xample Print E xample Print Example Print E xample üüüüüüüüüüü A ü & ü D Factory MODEL üüüüüü MX-50 Product S/N üüüüü P1234567 Serial nu mber ID üüüüüüü LAB-123 ID number . ＊ 1 PROGRAM üüüü No.
MS-70 / MX-50 / MF-50 / ML-50 47 10.1.3. 10.1.3. 10.1.3. 10.1.3. Expl Expl Expl Explanation for Pr int Item anation fo r Print Item anation fo r Print Item anation fo r Print Item "Analyzer infor.
MS-70 / MX-50 / MF-50 / ML-50 48 " " " "M e a s u r e m e n t Measur ement Measurement Measur ement Uni t" Unit" Uni t" Unit" Unit A Part of P rint Formula Dis .
MS-70 / MX-50 / MF-50 / ML-50 49 11. 11. 11. 11. Connecting to a Computer Connecting to a C omputer Connecting to a Computer Connecting to a C omputer The analy zer can be c onnected to perso nal c omputer using th e RS- 232C inter f ace. The analy zer is the Da ta Co mmuni cation Eq uipme nt type ( DCE).
MS-70 / MX-50 / MF-50 / ML-50 50 11.1. 11.1. 11.1. 11.1. RS RS RS RS - - - - 232C Seri al Int erfa ce 232C Seri al Int erfa ce 232C Seri al Int erfa ce 232C Seri al Int erfa ce RS RS RS RS - - - - 232.
MS-70 / MX-50 / MF-50 / ML-50 51 11.2. 11.2. 11.2. 11.2. Output Forma t Output Format Output Format Output Format In Case of F ormat omit te d Te mperature Da ta ( Functi on Table In Case of F ormat o.
MS-70 / MX-50 / MF-50 / ML-50 52 In Case of Format included Temperat ure Data (Function T able In Case of Format included Temperat ure Data (Function T able In Case of Format included Temperat ure Dat.
MS-70 / MX-50 / MF-50 / ML-50 53 12. 12. 12. 12. Data Memory Function Data Memory Function Data Memory Function Data Memory Function The data memory function automat ically stores each result when f inishing a measurement.
MS-70 / MX-50 / MF-50 / ML-50 54 12.1.2. 12.1.2. 12.1.2. 12.1.2. Output A ll Data at One Time Output All D ata at One Time Output All D ata at One Time Output All D ata at One Time 1. Display the gram u nit ( of the w eighing mode). 2. Press and h old the EN T ER k ey to display out .
MS-70 / MX-50 / MF-50 / ML-50 55 13. 13. 13. 13. Calibration Calibration Calibration Calibration The moist ure cont ent i s calcul ated w ith a rati o of w et wei ght and dried wei ght.
MS-70 / MX-50 / MF-50 / ML-50 56 13.2. 13.2. 13.2. 13.2. Calib Ca lib Ca lib Calib ration of the Weigh ting S enso r ration of the Weighting Sensor ration of the Weighting Sensor ration of the Weighting Sensor A stan dard mass o f 20g or 50g can be used for the c alibrati on A 20g st andar d mass ( AX-MX -41) i s recommend.
MS-70 / MX-50 / MF-50 / ML-50 57 Calibration R Calibration R Calibration R Calibration R eport eport eport eport Example for the Weighi Example for the W eighi Example for the Weighi Example for the W.
MS-70 / MX-50 / MF-50 / ML-50 58 13.3. 13.3. 13.3. 13.3. Calibratio n of Drying Temperatu re Calibratio n of Drying Temperatu re Calibratio n of Drying Temperatu re Calibratio n of Drying Temperatu re.
MS-70 / MX-50 / MF-50 / ML-50 59 10. After fifteen minutes, the buzzer sounds and the display blink s "1"6 "0 °C . Adjust the blinki ng v alue to th e the rmo mete r value us ing the ↓ or ↑ ke y .
MS-70 / MX-50 / MF-50 / ML-50 60 14. 14. 14. 14. Function Table Function Table Function Table Function Table The function t able can store the follow ing p arameter s to co ntrol the analy zer .
MS-70 / MX-50 / MF-50 / ML-50 61 14.1.1. 14.1.1. 14.1.1. 14.1.1. Operation Operation Operation Operation 1. Display the gram u nit ( of the w eighing mode). 2. Press and h old the SEL E C T key to enter th e function t able. Select an Item Select an Item Select an Item Select an Item 3.
MS-70 / MX-50 / MF-50 / ML-50 62 15. 15. 15. 15. Maintenance Maintena nce Maintena nce Maintena nce Turn off the powe r switch an d remo ve power cord du ring mai ntena nce . Coo l do wn all parts of t he analyze r bef ore ma intenanc e. P an su pport, samp le pan and br eeze b reak ring can be removed.
MS-70 / MX-50 / MF-50 / ML-50 63 15.2. 15.2. 15.2. 15.2. Replac ement of the Ha loge n Lamp Replacem ent of the Hal o gen La mp Replacem ent of the Hal o gen La mp Replacem ent of the Hal o gen La mp Replace the halogen lamp, when the dryin g time is exce ssive o r the lamp is def ective.
MS-70 / MX-50 / MF-50 / ML-50 64 15.3. 15.3. 15.3. 15.3. Factory Settings Factory Setti ngs Factory Setti ngs Factory Setti ngs This function c an set the follow ing p arameters to factory settings. All measure ment prog rams All results st ored i n memor y functi on.
MS-70 / MX-50 / MF-50 / ML-50 65 15.4. 15.4. 15.4. 15.4. Troubleshooting Troubleshooting Troubleshooting Troubleshooting １ １ １ １． ． ． ． In the Case tha t In the Case tha t In the Case .
MS-70 / MX-50 / MF-50 / ML-50 66 15.5. 15.5. 15.5. 15.5. Error Me ssage Error Mes sage Error Messa ge Error Mes sage CH no Internal Error An internal error indicated by the r esult o f the sel f-check functi on. If r epair is needed, co nt act the lo cal A&D dealer .
MS-70 / MX-50 / MF-50 / ML-50 67 16. 16. 16. 16. Specif ications Spec ifications Spec ifications Spec ifications MS-7 0 MX-5 0 MF-50 ML-5 0 Measurement method 400 W halogen lamp, thermogravimetric ana.
MS-70 / MX-50 / MF-50 / ML-50 68 MS-7 0 MX-5 0 MF-50 ML-5 0 Operation environment 5°C to 40°C (41 °F to 104°F ), 85%RH or less (no conden sation) Sample pan φ 85 mm Power sou rce, Maxim um cu rre nt (r .m.s) , Maximum consumption AC100V to 120V , 3A or AC200V to 240V , 1 .
MS-70 / MX-50 / MF-50 / ML-50 69 16.2. 16.2. 16.2. 16.2. Access orie s and Acces sor ie s and Acces sor ie s and Accessories and Peripheral Peri phera l Per ip hera l Peripheral Equ ipment Equipment E.
MS-70 / MX-50 / MF-50 / ML-50 70 17. 17. 17. 17. Ind ex Inde x Index Inde x %/min ---------------------------- 18, 2 1, 26 , 28 , ENTER ke y --------------------------- 13 , PROG RA M key ------------.
MS-70 / MX-50 / MF-50 / ML-50 71 ISO ------------------------------- 43, 56, 59, 6 0 Key mo de -------------------------------------- 6 0 Keys --------------------------------------------- 1 2 Levelin.
MS-70 / MX-50 / MF-50 / ML-50 72 MEMO.
MS-70 / MX-50 / MF-50 / ML-50 73.
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